Automatic Microreaction Hydrogenation Platform

Safer, More Efficient, and Energy-Saving Hydrogenation Process

Information

Automatic Microreaction Hydrogenation Platform
Micropacked bed technology significantly enhances the gas-liquid mass transfer coefficient, resulting in more compact equipment and intensifying the hydrogenation process. This advance greatly shortens reaction times.
The reactor has a small volume and includes inherent safety features.
For trace samples, the system can operate without passing through a gasliquid separator. Additionally, for fast sampling, a suitable gas-liquid separator can be selected based on application requirements to gather raw data for process scaling.
Three column sizes are available for selection: 6 mL, 10 mL, and 20 mL, making it suitable for both heterogeneous and homogeneous hydrogenation applications.
The system can operate at a maximum reaction temperature of 200 °C and a maximum pressure of 10 MPa, accommodating a wide range of hydrogenation needs.
This technology enables the rapid development of hydrogenation processes and efficient catalyst screening, improving overall process development.
The high-throughput version allows for the customization of kilogram-scale products.
The compact design allows the equipment to be placed in a fume hood for operation.
It is equipped with an inline UV and Fourier mid-infrared detector, enabling real-time monitoring and analysis.
The system integrates active safety protection schemes with passive measures, ensuring safer and more reliable operation of the instrument. 

Features

  • It can be connected directly to a hydrogen cylinder. You can also choose a high-pressure, high-purity hydrogen generator.

  • Full control over the entire hydrogenation process to avoid differences from batch to batch.

  • By shortening the reaction time to within 3 minutes, the hydrogenation process is improved.
  • The reactor is small, and the device is inherently safe.

  • It can screen conditions, prepare products on scales of milligrams and grams, and evaluate catalyst life.
  • A sampling port allows real-time sample collection.
  • The high-throughput version allows for kilogram-scale product preparation.

  • The instrument is small enough to fit in a fume hood.
  • With a maximum reaction temperature of 200℃ and a system working pressure of 10 MPa, it is suitable for a wide range of hydrogenation applications.

  • When combined with inline UV-visible and Fourier mid-infrared spectrometers, real-time inline monitoring and analysis are possible.
  • An optional inline automatic sample collector can save the trouble of manual sampling by collecting hydrogenation products at regular intervals.

Specifications

Model H-FLOW-S10 H-FLOW-H10 H-FLOW-S50
H-FLOW-H50
PumpDual-plunger high-pressure pump
No. of Liquid Pipeline1
No. of Gas Pipeline2
External Oil Bath ConnectorN/AR1/4 Male thread (standard), R1/4 Female thread and 10mm ferrule (optiona)
Material 316L C276 316L C276
System Resistance (Automatic BPV) ≤10 MPa (standard), 20 MPa (optional)
Working Pressure (Automatic BPV  ≤8 MPa (standard), 18 MPa (optional)
Reactor TemperatureRt-200℃
Catalyst Particle Size0.2-2 mm
Gas-Liquid Separator1 st degree separation
Liquid Feeding Flow Rate 0.0001-9.999 mL/min 0.1-50.0mL/min
Hydrogen Feeding Flow Rate 2-100 sccm
4-200 sccm
10-500 sccm
0.02-1 slm
Reaction Column Dimension Volume: 6 mL
ID: 6 mm
OD: 14 MM
Length: 212.5 mm
Volume: 150 mL
ID: 20 mm
OD: 29.5 MM
Length: 490 mm
Gas-Liquid Separator Volume 6 mL 100mL
Dimension (DxWxH, mm) 550x430x625600x484x725


Related Instruments

  • Chemistry-Related Product

    S-FLOW-100 Photochemistry Reaction Platform

    More Info
  • Chemistry-Related Product

    EMC-G2 Dual-Channel Catalyst Evaluation Device (Gas-Solid Reaction)

    More Info
  • Chemistry-Related Product

    The EMC-2 dual-channel automatic catalyst evaluation device is suitable for the development and screening stages of reactions. This device, employing microreaction technology at its core and automated process control,maximizes reaction efficiency. The fully-automated, compact system offers customizable configurations for catalyst screening. By executing a series of experiments through an interactive software control system, it yields high-precision and high reproducibility results in real time.

    More Info
  • Chemistry-Related Product

    The EMC-1 is a single-channel, fully automatic catalyst evaluation device designed for the catalyst development and screening stages. It significantly reduces time and labor requirements. This device utilizes microreaction technology at its core and is built on a fully automated process control system to ensure optimal reaction efficiency. Compact and innovative, the system offers a range of configurations and options for catalyst screening. Through an interactive software control system, it conducts a series of experiments that yield high-precision and reproducible results in real time.

    More Info
  • Chemistry-Related Product

    Automatic and Continuous Measurement of RTD Parameter

    More Info
  • Chemistry-Related Product

    The EMC-1 is a single-channel, fully automatic catalyst evaluation device designed for the catalyst development and screening stages. It significantly reduces time and labor requirements. This device utilizes microreaction technology at its core and is built on a fully automated process control system to ensure optimal reaction efficiency. Compact and innovative, the system offers a range of configurations and options for catalyst screening. Through an interactive software control system, it conducts a series of experiments that yield high-precision and reproducible results in real time.

    More Info

© Copyright 2024 FlowlabTech . All Rights Reserved.