Automatic Microreaction Hydrogenation Platform
Safer, More Efficient, and Energy-Saving Hydrogenation Process
Automatic Microreaction Hydrogenation Platform
Micropacked bed technology significantly enhances the gas-liquid mass transfer coefficient, resulting in more compact equipment and intensifying the hydrogenation process. This advance greatly shortens reaction times.
The reactor has a small volume and includes inherent safety features.
For trace samples, the system can operate without passing through a gasliquid separator. Additionally, for fast sampling, a suitable gas-liquid separator can be selected based on application requirements to gather raw data for process scaling.
Three column sizes are available for selection: 6 mL, 10 mL, and 20 mL, making it suitable for both heterogeneous and homogeneous hydrogenation applications.
The system can operate at a maximum reaction temperature of 200 °C and a maximum pressure of 10 MPa, accommodating a wide range of hydrogenation needs.
This technology enables the rapid development of hydrogenation processes and efficient catalyst screening, improving overall process development.
The high-throughput version allows for the customization of kilogram-scale products.
The compact design allows the equipment to be placed in a fume hood for operation.
It is equipped with an inline UV and Fourier mid-infrared detector, enabling real-time monitoring and analysis.
The system integrates active safety protection schemes with passive measures, ensuring safer and more reliable operation of the instrument.
Features
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It can be connected directly to a hydrogen cylinder. You can also choose a high-pressure, high-purity hydrogen generator.
- Full control over the entire hydrogenation process to avoid differences from batch to batch.
- By shortening the reaction time to within 3 minutes, the hydrogenation process is improved.
- The reactor is small, and the device is inherently safe.
- It can screen conditions, prepare products on scales of milligrams and grams, and evaluate catalyst life.
- A sampling port allows real-time sample collection.
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The high-throughput version allows for kilogram-scale product preparation.
- The instrument is small enough to fit in a fume hood.
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With a maximum reaction temperature of 200℃ and a system working pressure of 10 MPa, it is suitable for a wide range of hydrogenation applications.
- When combined with inline UV-visible and Fourier mid-infrared spectrometers, real-time inline monitoring and analysis are possible.
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An optional inline automatic sample collector can save the trouble of manual sampling by collecting hydrogenation products at regular intervals.
Specifications
| Model | H-FLOW-S10 | H-FLOW-H10 | H-FLOW-S50 |
H-FLOW-H50 |
| Pump | Dual-plunger high-pressure pump | |||
| No. of Liquid Pipeline | 1 | |||
| No. of Gas Pipeline | 2 | |||
| External Oil Bath Connector | N/A | R1/4 Male thread (standard), R1/4 Female thread and 10mm ferrule (optiona) | ||
| Material | 316L | C276 | 316L | C276 |
| System Resistance (Automatic BPV) | ≤10 MPa (standard), 20 MPa (optional) | |||
| Working Pressure (Automatic BPV | ≤8 MPa (standard), 18 MPa (optional) | |||
| Reactor Temperature | RT-200℃ | |||
| Catalyst Particle Size | 0.2-2 mm | |||
| Gas-Liquid Separator | 1 st degree separation | |||
| Liquid Feeding Flow Rate | 0.0001-9.999 mL/min | 0.1-50.0 mL/min | ||
| Hydrogen Feeding Flow Rate | 2-100 sccm 4-200 sccm 10-500 sccm 0.02-1 slm |
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| Reaction Column Dimension | Volume: 6 mL ID: 6 mm OD: 14 MM Length: 212.5 mm |
Volume: 150 mL ID: 20 mm OD: 29.5 MM Length: 490 mm |
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| Gas-Liquid Separator Volume | 6 mL | 100 mL |
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| Dimension (DxWxH, mm) | 550x430x625 | 600x484x725 | ||



